Items | Condition |
---|---|
Instrument | GC: HP 5890(Agilent Inc., Santa Clara, CA, USA) MS: HP 5973(Agilent Inc., Santa Clara, CA, USA) |
Column | DB-1MS, fused silica capillary column 30 m (length), 0.32 mm (i. d), 0.25 µm (film thick.) 0.25 µm (film thickness) |
Transfer temp. | 250°C |
Injector temp. | 320°C |
Flow rate | Helium 5 mL/min |
Column temp. | Programmed from 230 to 305°C, 3°C/min 305 to 320°C, 20°C/min |
MS quad. temp. | 150°C |
MS source temp. | 230°C |
Ionization | EI (70 eV) |