Table 2. Mean1) values for the reaction efficiency (RE), molar degree of substitution (MS), and resistant starch (RS) content of starch citrates prepared according to reaction conditions constructed by 23 full factorial design

Code Reaction condition RE (%) MS (×10-2) RS


Starch genotype pH T2) (°C) Uncooked (%, s.b3)) Cooked (%, s.b3))
N1 Normal 3.5 120 61.6±1.5d 2.4±0.0d 28.9±0.9c 27.3±0.2b
N2 Normal 3.5 150 90.7±0.7a 3.6±0.0b 40.6±0.1b 37.7±0.6a
N3 Normal 5.5 120 33.3±0.2f 0.3±0.0g 15.2±0.6f 12.3±0.5e
N4 Normal 5.5 150 72.6±3.3b 0.8±0.0e 16.8±0.3e 14.7±0.1d
W1 Waxy 3.5 120 67.8±0.2c 2.9±0.0c 27.5±0.7cd 25.8±0.2c
W2 Waxy 3.5 150 91.4±0.6a 3.9±0.0a 41.9±0.3a 37.7±0.6a
W3 Waxy 5.5 120 10.8±0.0g 0.1±0.0h 13.5±0.6g 10.1±0.2f
W4 Waxy 5.5 150 55.3±0.0e 0.4±0.0f 15.2±0.6f 12.2±0.5e
Mean value of three measurements; values within a column sharing the same lowercase letter are not significantly different (p<0.05).
Reaction temperature.
Dry starch weight basis.