입자 크기와 초고압 처리에 따른 유기용매와 초임계 유체 추출법에서의 대두유 추출수율의 변화
Received: Jan 12, 2011; Revised: Jun 25, 2011; Accepted: Jun 27, 2011
Published Online: Aug 31, 2011
Abatract
Effects of particle size and high pressure processing on the extraction rate of oil compounds from soybean powder were evaluated by Soxhlet method using hexane and supercritical fluid extraction (SFE) using CO2. SFE was carried out at 4,000 psi and 50°C for 4 hr. The mean particle sizes were varied from 26.7 to 862.0 μm by controlling milling time. Saturation solubility increased as the particle size decreased. At large particle size, high pressure processing (HPP) showed higher extraction yield in both hexane extraction and SFE, but as the particle size decreased, the HPP was irrelevant to the extraction yield in SFE. The higher extraction rate was obtained from the smaller particle size. The scanning electronic microscopy of soybean powder treated by HPP showed pores on the surface of the particle. The higher extraction rate and yield from HPP treatment might be due to the less internal resistance of transferring the solvent and miscellar in the solid matrix by collapsing of tissues.